DETERMINATION OF TELLURIUM IN URINE BY HYDRIDE GENERATION AND GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY-COMPARATIVE STUDY

GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY WITH MAlIlRIX MODIFICATION FOR DETERMINATION OF LEAD IN DRINKING WATER

An amoniumvanadate plus sodium molybdate mixed modifier Graphite Furnace Atomic Absorption Spectrometric method has been developed for determination of traces of lead in drinking water. The concentration of lead in the sample is obtained by direct comparison to linear working graph prepared from aqueous standards in the modifier medium, The results indicate the better performance of the pro...

Determination of trace selenium in urine by derivative hydride generation atomic absorption spectrometry.

Utilization of electrodeposition on a graphite probe modified with palladium in determination of lead by graphite furnace atomic absorption spectrometry in water and environmental samples

In this work a rapid and selective procedure for separation and preconcentration of lead(Pb2+) before determination by electrothermal atomic absorption spectrometry (ETAAS) wasdeveloped. The procedure is based on the electrodeposition on a graphite probe modified withpalladium. The lead was deposited from acetate buffer solution at pH 5.5. Various parameters,such as pH of solutions, deposition ...

Determination of cadmium in blood and urine by graphite furnace atomic absorption spectrophotometry.

カ ド ミウム(Cd)作 業者 のCd曝 露 指 標 として,血 液 お よび 尿 中Cdの 測 定 が有 効 であ り1),こ れ ら生体 試 料 中 のCd測 定方 法 と しては黒 鉛 炉原 子 吸 光法2~6)が 広 く 用 い られ て い る.こ の方 法 に よるCd定 量 では, Cdお よび そ の化合 物 の融点 が低 いた め,原 子 化 段階 以 前 での 揮 散 が問 題 で あ り,対 策 と して適 当な 干渉 抑制 剤 を添 加 す る ことに よ り,揮 散 を 抑制 す る方 法 が と られ て い る. Cd定 量 に 対 して は, HNO32-4), NH4H2PO43,4), NH4NO33-5), NH4F4,6)お よびPd(NO3)25)な どが 干渉 抑制 剤 と して提 唱 され て い る.血 中Cd(Cd-B)の 定量 に従...

Determination and Levels of Chromium in French Wine and Grapes by Graphite Furnace Atomic Absorption Spectrometry

An accurate and precise method for direct determination of chromium in wine using graphite furnace atomic absorption spectrometry (GFAAS) is described. The method was also applied to grape samples treated by previous acid mineralization. A total of 79 wine samples from different regions in France and 12 grape samples of different varieties were analyzed. Chromium levels ranged from 7.0 to 90.0 ...